Revealing Intrinsic Functionalization, Structure, and Photo‐Thermal Oxidation in Hexagonal Antimonene (Small 25/2026)

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Hexagonal Antimonene Thiol-functionalized β-antimonene hexagons produced by colloidal synthesis are illuminated by a probing laser beam. Raman thermometry reveals thickness-dependent heating and surface oxidation, while surface thiols preserve the crystalline core, enabling controlled antimony/antimony-oxide interfaces in 2D materials. More in the Research Article (2404319), Gonzalo Abellán and co-workers.