A Catalyst-Coated Mesoporous Carbon–Membrane Electrode Assembly for In-situ Soft X-ray XPS and NEXAFS Studies of Electrocatalytic Interfaces
James J. C. Counter, Santosh Kumar, Christopher M. Zalitis, Mark Clapp et autres
In-situ soft X-ray spectroscopy provides direct insight into the electronic structure of electrocatalysts under realistic reaction conditions but remains technically challenging due to the need to combine aqueous electrochemistry with ultra-high-vacuum detection. Here we present a mesoporous carbon–membrane working electrode assembly (WEA) …
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